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Evolved gas analysis /

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Focuses on so-called 'hyphenated techniques' (EGA-TGA, TGA-GC/MS, etc), which allow a great deal of chemical information about a sample to be revealed quickly and conveniently. The methods are highly applicable to polymer/plastics samples, but also to other materials including pharmaceutic...

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Bibliographic Details
Main Author: Fedelich, Nicolas, 1978- (Author)
Corporate Author: Knovel (Firm)
Format: eBook
Language:English
Published: Cincinnati : Hanser Publications, [2019]
Subjects:
Gases > Analysis.
Gaz > Analyse.
Gases > Analysis
Electronic books.
Online Access:Connect to the full text of this electronic book
Table of Contents:
  • Intro
  • Preface
  • Contents
  • 1 Introduction to Evolved Gas Analysis
  • 2 TGA-MS
  • 2.1 Principles of MS
  • 2.2 The TGA-MS System
  • 2.3 Measurement Modes
  • 2.4 Interpretation of Results
  • 2.5 Typical Fragmentation Patterns
  • 2.6 Presentation of Results
  • 3 TGA-FTIR
  • 3.1 Principles of FTIR
  • 3.2 The TGA-FTIR System
  • 3.3 Presentation of Results
  • 3.4 Interpretation Procedure
  • 3.5 Interpretation of Spectra
  • 3.6 Characteristic Absorption Frequencies
  • 3.7 Presentation of Results
  • 4 TGA-GC/MS
  • 4.1 Principles of GC
  • 4.2 The TGA-GC/MS System
  • 4.3 Measurement Possibilities
  • 4.4 Results
  • 5 TGA-Micro GC/MS
  • 5.1 Principles of Micro GC
  • 5.2 TGA-Micro GC and TGA-Micro GC/MS Systems
  • 5.3 Results
  • 6 Introduction to the Applications
  • 7 Applications List
  • 7.1 Decomposition of Calcium Oxalate Monohydrate (Tutorial) by TGA-MS, TGA-FTIR and TGA-Micro GC
  • 7.2 Decomposition of Copper Sulfate Pentahydrate (Tutorial) by TGA-MS and TGA-FTIR
  • 7.3 Influence of Experimental Conditions on MS Sensitivity
  • 7.4 Decomposition of Acetylsalicylic Acid by TGA-MS and TGA-GC/MS Multi-injection
  • 7.5 Thermal Degradation of BHET by TGA-FTIR
  • 7.6 Decomposition of Technical Lauryl Alcohol by TGA-FTIR
  • 7.7 Detection of Residual Solvents in a Pharmaceutical Substance by TGA-MS
  • 7.8 Desorption of a Zeolite Filled with Organic Matter by TGA-MS
  • 7.9 Pyrolysis of PVC Powder by TGA-MS
  • 7.10 Investigation of Fluorinated Cable Wires by TGA-FTIR
  • 7.11 Detection of Methyl Salicylate in a Rubber Sample by TGA-MS
  • 7.12 Degradation of a Silicone Polymer by TGA-FTIR
  • 7.13 Curing and Decomposition of an Amino Resin by TGA-MS and TGA-FTIR
  • 7.14 Identification of BR and NR Rubbers. Study of Thermal Transitions and Decomposition by TGA-FTIR and DSC
  • 7.15 Delamination of Printed Circuit Boards by TMA-MS.
  • 7.16 Expansion and Decomposition of a Polymer Used To Encapsulate a Blowing Agent by TMA-MS
  • 7.17 Determination of the Water Content of an Ionic Liquid by TGA-MS
  • 7.18 From the Investigation of Pyrolysis to the Elucidation of Fire Retardancy Mechanisms by TGA-FTIR
  • 7.19 High Melting Ceramics by TGA-MS and DSC
  • 7.20 Thermal Behavior of Zoledronic Acid Hydrate by TGA-MS and DSC-Microscopy
  • 7.21 Quantification of Cobalt Oxide in a Coated Cobalt Powder by TGA-MS
  • 7.22 Investigation of Evolved Decomposition Products of Polyamide 66 by TGA-GC/MS and TGA-Micro GC/MS
  • 7.23 Identification of Multi-Component Thermoplastics by TGA-GC/MS, DSC and DMA
  • 7.24 Deformulation of a Rubber by TGA-GC/MS, DSC, DMA and ATR
  • 7.25 Polypropylene with and without Ammonium Phosphate Flame Retardant by TGA-GC/MS-FTIR
  • 7.26 Thermal Oxidation of EPDM Rubber by TGA-GC/MS
  • 7.27 Quantification of Dimethylformamide in Coatings by TGA-MS and TGA-GC/MS
  • 7.28 Quantification of a Low Content of Styrene-Butadiene Rubber in Natural Rubber by TGA-GC/MS
  • 7.29 Evolved Decomposition Products of a Phenol-Formaldehyde Resin by TGA-Micro GC/MS
  • 7.30 Quantification of Carbon Dioxide in a Coke Sample by TGA-Micro GC/MS
  • 7.31 Synthesis and Characterization of Barium Titanate by TGA-Micro GC/MS, TMA and DSC
  • 7.32 Determination of Water Content in a Thermoplastic by TGA-Micro GC/MS and Karl Fischer titrator
  • 7.33 Study of a Biomass Sample by TGA-GC/MS and TGA-Micro GC/MS
  • 7.34 Gases Evolved from Lignite by TGA-GC/MS and TGA-Micro GC/MS
  • 8 Literature
  • 9 Units, Abbreviations and Acronyms
  • 10 Index.