Evolved gas analysis /

Focuses on so-called 'hyphenated techniques' (EGA-TGA, TGA-GC/MS, etc), which allow a great deal of chemical information about a sample to be revealed quickly and conveniently. The methods are highly applicable to polymer/plastics samples, but also to other materials including pharmaceutic...

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Bibliographic Details
Main Author: Fedelich, Nicolas, 1978- (Author)
Corporate Author: Knovel (Firm)
Format: eBook
Language:English
Published: Cincinnati : Hanser Publications, [2019]
Subjects:
Online Access:Connect to the full text of this electronic book

MARC

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100 1 |a Fedelich, Nicolas,  |d 1978-  |e author.  |1 https://id.oclc.org/worldcat/entity/E39PCjHg9dRWCKgDQxWFHQ3PHy 
245 1 0 |a Evolved gas analysis /  |c Nicolas Fedelich. 
264 1 |a Cincinnati :  |b Hanser Publications,  |c [2019] 
300 |a 1 online resource 
336 |a text  |b txt  |2 rdacontent 
337 |a computer  |b c  |2 rdamedia 
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504 |a Includes bibliographical references and index. 
588 0 |a Online resource; title from digital title page (viewed on March 02, 2020). 
505 0 |a Intro -- Preface -- Contents -- 1 Introduction to Evolved Gas Analysis -- 2 TGA-MS -- 2.1 Principles of MS -- 2.2 The TGA-MS System -- 2.3 Measurement Modes -- 2.4 Interpretation of Results -- 2.5 Typical Fragmentation Patterns -- 2.6 Presentation of Results -- 3 TGA-FTIR -- 3.1 Principles of FTIR -- 3.2 The TGA-FTIR System -- 3.3 Presentation of Results -- 3.4 Interpretation Procedure -- 3.5 Interpretation of Spectra -- 3.6 Characteristic Absorption Frequencies -- 3.7 Presentation of Results -- 4 TGA-GC/MS -- 4.1 Principles of GC -- 4.2 The TGA-GC/MS System -- 4.3 Measurement Possibilities -- 4.4 Results -- 5 TGA-Micro GC/MS -- 5.1 Principles of Micro GC -- 5.2 TGA-Micro GC and TGA-Micro GC/MS Systems -- 5.3 Results -- 6 Introduction to the Applications -- 7 Applications List -- 7.1 Decomposition of Calcium Oxalate Monohydrate (Tutorial) by TGA-MS, TGA-FTIR and TGA-Micro GC -- 7.2 Decomposition of Copper Sulfate Pentahydrate (Tutorial) by TGA-MS and TGA-FTIR -- 7.3 Influence of Experimental Conditions on MS Sensitivity -- 7.4 Decomposition of Acetylsalicylic Acid by TGA-MS and TGA-GC/MS Multi-injection -- 7.5 Thermal Degradation of BHET by TGA-FTIR -- 7.6 Decomposition of Technical Lauryl Alcohol by TGA-FTIR -- 7.7 Detection of Residual Solvents in a Pharmaceutical Substance by TGA-MS -- 7.8 Desorption of a Zeolite Filled with Organic Matter by TGA-MS -- 7.9 Pyrolysis of PVC Powder by TGA-MS -- 7.10 Investigation of Fluorinated Cable Wires by TGA-FTIR -- 7.11 Detection of Methyl Salicylate in a Rubber Sample by TGA-MS -- 7.12 Degradation of a Silicone Polymer by TGA-FTIR -- 7.13 Curing and Decomposition of an Amino Resin by TGA-MS and TGA-FTIR -- 7.14 Identification of BR and NR Rubbers. Study of Thermal Transitions and Decomposition by TGA-FTIR and DSC -- 7.15 Delamination of Printed Circuit Boards by TMA-MS. 
505 8 |a 7.16 Expansion and Decomposition of a Polymer Used To Encapsulate a Blowing Agent by TMA-MS -- 7.17 Determination of the Water Content of an Ionic Liquid by TGA-MS -- 7.18 From the Investigation of Pyrolysis to the Elucidation of Fire Retardancy Mechanisms by TGA-FTIR -- 7.19 High Melting Ceramics by TGA-MS and DSC -- 7.20 Thermal Behavior of Zoledronic Acid Hydrate by TGA-MS and DSC-Microscopy -- 7.21 Quantification of Cobalt Oxide in a Coated Cobalt Powder by TGA-MS -- 7.22 Investigation of Evolved Decomposition Products of Polyamide 66 by TGA-GC/MS and TGA-Micro GC/MS -- 7.23 Identification of Multi-Component Thermoplastics by TGA-GC/MS, DSC and DMA -- 7.24 Deformulation of a Rubber by TGA-GC/MS, DSC, DMA and ATR -- 7.25 Polypropylene with and without Ammonium Phosphate Flame Retardant by TGA-GC/MS-FTIR -- 7.26 Thermal Oxidation of EPDM Rubber by TGA-GC/MS -- 7.27 Quantification of Dimethylformamide in Coatings by TGA-MS and TGA-GC/MS -- 7.28 Quantification of a Low Content of Styrene-Butadiene Rubber in Natural Rubber by TGA-GC/MS -- 7.29 Evolved Decomposition Products of a Phenol-Formaldehyde Resin by TGA-Micro GC/MS -- 7.30 Quantification of Carbon Dioxide in a Coke Sample by TGA-Micro GC/MS -- 7.31 Synthesis and Characterization of Barium Titanate by TGA-Micro GC/MS, TMA and DSC -- 7.32 Determination of Water Content in a Thermoplastic by TGA-Micro GC/MS and Karl Fischer titrator -- 7.33 Study of a Biomass Sample by TGA-GC/MS and TGA-Micro GC/MS -- 7.34 Gases Evolved from Lignite by TGA-GC/MS and TGA-Micro GC/MS -- 8 Literature -- 9 Units, Abbreviations and Acronyms -- 10 Index. 
520 |a Focuses on so-called 'hyphenated techniques' (EGA-TGA, TGA-GC/MS, etc), which allow a great deal of chemical information about a sample to be revealed quickly and conveniently. The methods are highly applicable to polymer/plastics samples, but also to other materials including pharmaceuticals, biomass, and various organic and inorganic compounds. 
650 0 |a Gases  |x Analysis. 
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