Contemporary practice of chromatography /
Written for all those who use chromatography as an analytical tool, this book covers all areas of gas, liquid, and thin-layer chromatography; no other book offers the same scope. The authors have had considerable experience in teaching graduate-level courses and the material presented here has been...
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| Format: | eBook |
| Language: | English |
| Language Notes: | English. |
| Published: |
Amsterdam ; New York :
Elsevier,
1984.
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| Series: | Developments in mineral processing Gravity concentration technology
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| Subjects: | |
| Online Access: | Connect to the full text of this electronic book |
Table of Contents:
- Front Cover; Contemporary Practice of Chromatography; Copyright Page; Table of Contents; Preface; CHAPTER 1. FUNDAMENTAL RELATIONSHIPS OF CHROMATOGRAPH; 1.1 Introduction; 1.2 Retention; 1.3 Flow in Porous Media; 1.4 Band Broadening Mechanisms; 1.5 Parameters Affecting Resolution; 1.6 Peak Shape Models; 1.7 Retention Index Systems; 1.8 References; CHAPTER 2. THE COLUMN IN GAS CHROMATOGRAPHY; 2.1 Introduction; 2.2 Gas-Liquid Chromatography; 2.3 Preparation of Packed Columns; 2.4 Performance Evaluation of Packed Columns
- 2.5 Contribution of Interfacial Adsorption to Retention in Gas-Liquid Chromatography2.6 Bonded Liquid Phases; 2.7 Porous Polymer Beads; 2. 8 Gas-Solid Chromatography; 2.9 Micropacked Columns; 2.10 Open Tubular Columns; 2.11 Evaluation of the Quality of Open Tubular Columns; 2.12 The Mobile Phase in Gas Chromatography; 2.13 Supercritical Fluid Chromatography; 2.14 References; CHAPTER 3. INSTRUMENTAL REQUIREMENTS FOR GAS CHROMATOGRAPHY; 3.1 Introduction; 3.2 Syringe Injection Techniques; 3.3 In jection Devices for Open Tubular Capillary Columns; 3.4 Detection Devices for Gas Chromatography
- 3.5 Column Effluent Splitters for Parallel Detection3. 6 Multidimensional Gas Chromatography; 3.7 Temperature and Flow Programming; 3.8 References; CHAPTER 4. THE COLUMN IN LIQUID CHROMATOGRAPHY; 4.1 Introduction; 4.2 Selection of the Separation Method; 4,3 Column Packing Materials for HPLC; 4.4 Column Preparation; 4.5 Column Testing and Evaluation; 4,6 Radial Compression Columns; 4.7 Guard Columns; 4.8 Mobile Phase Selection in HPLC; 4.9 Gradient Elution in Liquid Chromatography; 4.10 Liquid-Solid Chromatography; 4.11 Polar Bonded Phases; 4.12 Reversed-Phase Chromatography
- 4.13 Size-Exclusion Chromatography4.14 Ion-Exchange Chromatography; 4.15 Ion Chromatography; 4.16 Microcolumns in Liquid Chromatography; 4.17 High Speed Liquid Chromatography; 4.18 Multidimensional Liquid Chromatography; 4.19 Temperature and Flow Programming in Liquid Chromatography; 4.20 References; CHAPTER 5. INSTRUMENTAL REQUIREMENTS FOR HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; 5.1 Introduction; 5.2 Equipment Specifications; 5.3 Solvent Reservoirs and Solvent Degassing; 5. 4 High Pressure Pumps; 5.5 Gradient Devices; 5.6 Injection Devices; 5.7 Detectors for Liquid Chromatography
- 5.8 Data Acquisition and Signal Processing5.9 Quantitative Analysis; 5.10 References; CHAPTER 6. PREPARATIVE-SCALE CHROMATOGRAPHY; 6.1 Introduction; 6.2 Gas Chromatography; 6.3 Low
- and Medium-Pressure Liquid Chromatography; 6.4 High-Pressure Liquid Chromatography; 6.5 Countercurrent Chromatography; 6.6 References; CHAPTER 7. SAMPLE PREPARATION FOR CHROMATOGRAPHCI ANALYSIS; 7.1 Introduction; 7.2 Isolation and Concentration Techniques using Physical Methods; 7.3 Isolation and Concentration Techniques using Solvent Extraction; 7.4 Sample Cleanup Using Liquid-Solid Chromatography