http://www.loc.gov/mods/v3 http://www.loc.gov/standards/mods/v3/mods-3-2.xsd
Written for all those who use chromatography as an analytical tool, this book covers all areas of gas, liquid, and thin-layer chromatography; no other book offers the same scope. The authors have had considerable experience in teaching graduate-level courses and the material presented here has been tried and tested, having formed the basis for short courses taught to groups of industrial chemists. Emphasis is on the practice of chromatographic methods, including ``how to'' sections and numerous examples of calculation methods. Extensively illustrated, the book contains numerous tables of all useful constants, materials and formulas frequently used by chromatographers. Valuable features are the chapters on sample preparation for chromatographic analysis, on instrumental methods for sample identification, and the comprehensive literature review.
Front Cover; Contemporary Practice of Chromatography; Copyright Page; Table of Contents; Preface; CHAPTER 1. FUNDAMENTAL RELATIONSHIPS OF CHROMATOGRAPH; 1.1 Introduction; 1.2 Retention; 1.3 Flow in Porous Media; 1.4 Band Broadening Mechanisms; 1.5 Parameters Affecting Resolution; 1.6 Peak Shape Models; 1.7 Retention Index Systems; 1.8 References; CHAPTER 2. THE COLUMN IN GAS CHROMATOGRAPHY; 2.1 Introduction; 2.2 Gas-Liquid Chromatography; 2.3 Preparation of Packed Columns; 2.4 Performance Evaluation of Packed Columns
2.5 Contribution of Interfacial Adsorption to Retention in Gas-Liquid Chromatography2.6 Bonded Liquid Phases; 2.7 Porous Polymer Beads; 2. 8 Gas-Solid Chromatography; 2.9 Micropacked Columns; 2.10 Open Tubular Columns; 2.11 Evaluation of the Quality of Open Tubular Columns; 2.12 The Mobile Phase in Gas Chromatography; 2.13 Supercritical Fluid Chromatography; 2.14 References; CHAPTER 3. INSTRUMENTAL REQUIREMENTS FOR GAS CHROMATOGRAPHY; 3.1 Introduction; 3.2 Syringe Injection Techniques; 3.3 In jection Devices for Open Tubular Capillary Columns; 3.4 Detection Devices for Gas Chromatography
3.5 Column Effluent Splitters for Parallel Detection3. 6 Multidimensional Gas Chromatography; 3.7 Temperature and Flow Programming; 3.8 References; CHAPTER 4. THE COLUMN IN LIQUID CHROMATOGRAPHY; 4.1 Introduction; 4.2 Selection of the Separation Method; 4,3 Column Packing Materials for HPLC; 4.4 Column Preparation; 4.5 Column Testing and Evaluation; 4,6 Radial Compression Columns; 4.7 Guard Columns; 4.8 Mobile Phase Selection in HPLC; 4.9 Gradient Elution in Liquid Chromatography; 4.10 Liquid-Solid Chromatography; 4.11 Polar Bonded Phases; 4.12 Reversed-Phase Chromatography
4.13 Size-Exclusion Chromatography4.14 Ion-Exchange Chromatography; 4.15 Ion Chromatography; 4.16 Microcolumns in Liquid Chromatography; 4.17 High Speed Liquid Chromatography; 4.18 Multidimensional Liquid Chromatography; 4.19 Temperature and Flow Programming in Liquid Chromatography; 4.20 References; CHAPTER 5. INSTRUMENTAL REQUIREMENTS FOR HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; 5.1 Introduction; 5.2 Equipment Specifications; 5.3 Solvent Reservoirs and Solvent Degassing; 5. 4 High Pressure Pumps; 5.5 Gradient Devices; 5.6 Injection Devices; 5.7 Detectors for Liquid Chromatography
5.8 Data Acquisition and Signal Processing5.9 Quantitative Analysis; 5.10 References; CHAPTER 6. PREPARATIVE-SCALE CHROMATOGRAPHY; 6.1 Introduction; 6.2 Gas Chromatography; 6.3 Low -- and Medium-Pressure Liquid Chromatography; 6.4 High-Pressure Liquid Chromatography; 6.5 Countercurrent Chromatography; 6.6 References; CHAPTER 7. SAMPLE PREPARATION FOR CHROMATOGRAPHCI ANALYSIS; 7.1 Introduction; 7.2 Isolation and Concentration Techniques using Physical Methods; 7.3 Isolation and Concentration Techniques using Solvent Extraction; 7.4 Sample Cleanup Using Liquid-Solid Chromatography
Includes bibliographical references and index.
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