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Monographs in Organic Functional Group Analysis, Volume 4: The Determination of Organic Peroxides focuses on the analytical chemistry of organic peroxides. The monograph first offers information on the compositions, properties, and reactions of lipid peroxides, polymers, and petrochemicals. The text then reviews the iodometric methods, including choice of solvents, reaction conditions, and titration with thiosulfate. The ferrous ion methods are also discussed. Considerations include choice of reagents and solvents and titration with titanous, dichromate, and mercurous ions. The book also focus.
Front Cover; The Determination of Organic Peroxides; Copyright Page; Table of Contents; PREFACE; CHAPTER 1. INTRODUCTION; 1. Lipid Peroxides; 2 . Polymers; 3 . Petrochemicals; 4 . Irradiation; 5. Miscellaneous; References; CHAPTER 2 . STRUCTURE AND REACTIVITY; 1 . Classification of peroxides; 2 . Reactivity; References; CHAPTER 3. IODOMETRIC METHODS; 1 . General comments; 2. Choice of solvent; 3 . Reaction conditions; 4 . Titration with thiosulphate; References; CHAPTER 4 . FERROUS ION METHODS; 1 . Introduction; 2 . Choice of reagent; 3. Choice of solvent; 4 . Titration with titanous ions
5 . Titration with dichromate ions6 . Titration with mercurous ions; References; CHAPTER 5. FURTHER TITRIMETRIC REAGENTS; 1 . Introduction; 2 . Arsenious methods; 3 . Stannous methods; 4 . Titanous methods; 5 . Titration with anions; 6. Sulphides and mercaptans; References; CHAPTER 6 . COLORIMETRIC METHODS; 1 . Introduction; 2 . Ferrous ions; 3 . Leuco base of methylene blue; 4 . Iodine; 5. iV, A^'-Dimethyl-/?-phenylenediamme; 6. Other colorimetric reagents; References; CHAPTER 7 . POLAROGRAPHIC METHODS; 1 . Introduction; 2 . Electrode reaction; 3 . Polarographic teclmiques for peroxides
4 . Nature and concentration of peroxide5 . Solvents and supporting electrolytes; References; CHAPTER 8. SPECTROSCOPIC TECHNIQUES; 1 . Introduction; 2 . Ultraviolet and visible absorption; 3 . Infrared absorption; 4 . Raman spectroscopy; References; CHAPTER 9 . CHROMATOGRAPHIC METHODS A. COLUMN CHROMATOGRAPHY; 1 . Introduction; 2 . Column techniques; 3 . Solvent medium; 4 . Stationary phase; 5 . Type of peroxide; References; CHAPTER 10 . CHROMATOGRAPHIC METHODS B. PAPER CHROMATOGRAPHY; 1 . Introduction; 2 . Choice of paper; 3. Mobile phase; 4 . General techniques; 5 . Chemical structure
6 . Detection7 . Class of peroxide; References; CHAPTER 11 . CHROMATOGRAPHIC METHODS C. THIN-LAYER CHROMATOGRAPHY; 1 . Introduction; 2 . Adsorbents; 3 . Solvent systems; 4. Detection; 5. Techniques; 6. Applications; References; CHAPTER 12. CHROMATOGRAPHIC METHODS D. GAS CHROMATOGRAPHY; 1. Introduction; 2. Solid support; 3. Stationary phase; 4. Column temperature; 5. Functional groups; 6. Quantitative analysis; References; CHAPTER 13. CHOICE OF METHOD; 1. Introduction; 2. Concentration of peroxide; 3. Reactivity of peroxide; 4. Nature of the sample; INDEX
Includes bibliographical references at the end of each chapters and index.
Monographs in organic functional group analysis ; Volume 4