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Annual Reports on NMR Spectroscopy provides a thorough and in-depth accounting of progress in nuclear magnetic resonance (NMR) spectroscopy and its many applications. Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained as much significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required, and in which the nature of interactions and reactions in solution is being studied. This book has established itself as a premier means for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy.
Front Cover -- Annual Reports on NMR Spectroscopy -- Copyright -- Contents -- Contributors -- Preface -- Chapter One: Solid-State NMR Studies of Lithium Ion Dynamics Across Materials Classes -- 1. Introduction -- 1.1. Diffusion: Lithium in Solids -- 1.2. Basics of Diffusion in Solid State -- 1.3. Li Nuclear Magnetic Resonance -- 2. Methods -- 2.1. Spin Relaxation NMR -- 2.2. Beta-NMR -- 2.3. Field Gradient NMR -- 2.4. Exchange NMR Spectroscopy -- 2.5. Spin Alignment Echo NMR -- 3. Application of NMR Methods in Materials -- 3.1. Hydrides -- 3.2. Oxides -- 3.3. Chalcogenides -- 3.4. Sulfates -- 3.5. Aluminates -- 3.6. Nitrides -- 3.7. Carbides -- 3.8. Silicides -- 3.9. Silicates -- 3.10. Halides -- 3.11. Transition Metal Oxides -- 3.11.1. Titanates -- 3.11.2. Vanadates -- 3.11.3. Niobates -- 3.11.4. Oxides of Co and Mn -- 3.11.5. Oxides of Ta and Zr -- 3.12. Transition Metal Chalcogenides -- 3.13. Transition Metal Phosphates -- 3.14. Garnets -- 3.15. Other Inorganic Compounds -- 3.16. Zeolites -- 3.17. Metallic Lithium -- 3.18. Glasses -- 3.18.1. Chalcogenide Glasses -- 3.18.2. Borate Glasses -- 3.18.3. Phosphate Glasses -- 3.18.4. Silicate Glasses -- 3.18.5. Mixed Glasses -- 3.19. Polymers -- 3.20. Organic Solids -- 4. Conclusions -- Acknowledgments -- References -- Chapter Two: Orphan Spin Polarization: A Catalyst for High-Throughput Solid-State NMR Spectroscopy of Proteins -- 1. Introduction -- 2. Single and Multiple Acquisition MAS Solid-State NMR -- 3. Dual Polarization Pathways and Simultaneous Acquisition of Multidimensional Experiments -- 4. Deconvolution of Transferred and Residual Polarization Pathways Enables the Acquisition of Multiple Two- and Three-Dime ... -- 5. How Far Can We Push the Residual Polarization? -- 6. Strategies for Choosing the Best Scheme for Simultaneous Acquisition of ssNMR Experiments -- 7. Conclusions and Outlook.
Acknowledgments -- References -- Chapter Three: Analytic Theory of Multiple-Quantum NMR of Quadrupolar Nuclei -- 1. Introduction -- 2. Theory and Discussion -- 2.1. Excitation in MQ Experiments -- 2.2. Evolution of Coherences (Indirect Dimension) -- 2.3. Reconversion of MQ Coherences -- 2.3.1. Single-Pulse Method -- 3. Z-Filter Method -- 4. Conclusions -- Acknowledgments -- Appendix A -- A.1. Representation of Quadrupolar Interactions -- Appendix B -- Appendix C -- C.1. Phase-Cycling Schemes for Two-Pulse MQ Experiments -- C.2. Phase-Cycling Schemes for Three-Pulse MQ Experiments (Z-Filter) -- References -- Chapter Four: Recent Advances in NMR Studies of Carbohydrates -- 1. Introduction -- 2. Experimental NMR Methods -- 2.1. One-Dimensional NMR Experiments -- 2.2. Two- and Multidimensional NMR Experiments -- 2.3. Diffusion-Ordered Spectroscopy -- 2.4. Solid-State NMR -- 2.5. Multidimensional NMR Spectrum -- 2.6. Paramagnetism-Assisted NMR of Oligosaccharides -- 3. Noncovalent Interaction Studied by NMR -- 3.1. Sugar-Protein Interaction -- 3.2. Other Sugar Complexes -- 4. Structural and Conformational Analysis of Saccharides -- 4.1. Monosaccharides and Their Derivatives -- 4.2. Oligo- and Polysaccharides -- 5. Mechanistic Investigations -- 6. NMR Development in Carbohydrate Impurities Profiling -- 7. Computational NMR Methods -- 7.1. Force Fields -- 7.2. Computational NMR of Carbohydrates -- 7.3. CASPER Approach -- References -- Index -- Back Cover.
Includes bibliographical references and index.
Spectroscopie de la résonance magnétique nucléaire
Annual reports on NMR spectroscopy. Volume eighty nine
Annual reports on NMR spectroscopy ; v. 89