Forensic applications of high performance liquid chromatography /
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| Format: | eBook |
| Language: | English |
| Language Notes: | English. |
| Published: |
Boca Raton :
CRC Press/Taylor & Francis,
©2010.
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| Series: | Analytical Concepts in Forensic Chemistry.
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| Subjects: | |
| Online Access: | Connect to the full text of this electronic book |
Table of Contents:
- Introduction to HPLC The History of Chromatography; Basic Instrumentation
- Basic Principles of HPLC: Theory of Chromatography; Chemical Bonding and Polarity
- Mobile Phase Preparation, the Use of Buffers, and Sample Preparation: Mobile Phase Preparation; Buffers; Sample and Standard Preparation
- Modes of Separation: Reverse Phase HPLC; Ion Exchange; Normal Phase HPLC
- Detection Systems: Theory; UV/Vis Detectors versus Diode Array Detectors; Electrochemical Detectors; Mass Spectrometry
- Method Development in Reversed Phase HPLC: Sample Composition; Which Column Will Affect the Separation?; Choosing a Mobile Phase; Automated Method Development; Method Development Strategy; Method Development Worked Example
- System Suitability
- System Performance; Chromatographic Suitability
- Qualification, Validation, and Verification: Valid Analytical Measurement ; Estimation of Uncertainty of Measurement, Sources of Error, and Statistical Evaluation; Instrument Qualification; Method Validation; Method Verification
- Quality Systems: What Is Quality?; Introduction to Quality Assurance; How Do We Ensure Quality in Our Laboratories?; A Quality Management System; Accreditation; Auditing
- Troubleshooting HPLC Systems: Troubleshooting; Tool Kit and Spare Parts; Preventative Maintenance; Column Care
- Forensic Applications of HPLC: Drug Analysis; Toxicological Analysis; Colour Analysis; Analysis of Explosives; Food and the Environment.