Table of Contents:
  • Machine derived contents note: Preface ix
  • 1. Reflections on Process Research 1
  • Edward J.J. Grabowski
  • 2. Synthesis of Cell Adhesion Inhibitors via
  • Crystallization-Driven Dynamic Transformations 23
  • Magnus Eriksson, Vittorio Farina, Suresh Kapadia,
  • Elio Napolitano, and Nathan K. Yee
  • 3. Synthetic, Structural, and Mechanistic Issues in the Development of a Subtype Selective GABA
  • Partial Agonist Hypnotic Agent 39
  • John A. Ragan, Jerry A. Murry, Michael J. Castaldi,
  • Alyson K. Conrad, Paul D. Hill, Brian P. Jones,
  • Narasimhan Kasthurikrishnan, Bryan Li, Teresa W. Makowski,
  • Ruth McDermott, Barb J. Sitter, Timothy D. White,
  • and Gregory R. Young
  • 4. Process Research and Initial Scale-Up of ABT-839:
  • A Farnesyltransferase Inhibitor 59
  • Todd S. McDermott, Ramiya Premchandron, Anne E. Bailey,
  • Lakshmi Bhagavatula, and Howard E. Morton
  • 5. Synthetic Approaches to the Retinoids 71
  • Margaret M. Faul
  • 6. Design of Experiments in Pharmaceutical Process Research and
  • Development 87
  • John E. Mills
  • 7. Process Development for the MMP Inhibitor AG3433 111
  • Jayaram K. Srirangam, Ming Guo, Shu Yu, Alan W. Grubbs,
  • James Saenz, Steven L. Bender, Judith G. Deal, Kuenshan S. Lee,
  • Jason Liou, Robert Szendroi, James Faust, and Kim Albizati
  • 8. Dihydro-7-benzofurancarboxylic Acid: An Intermediate
  • in the Synthesis of the Enterokinetic Agent R108512 125
  • Bert Willemsens, Alex Copmans, Dirk Beerens, Stef Leurs,
  • Dirk de Smaele, Max Rey, and Silke Farkas
  • 9. Process Research Leading to an Enantioselective
  • Synthesis of a 5-Lipoxygenase Inhibitor for Asthma 141
  • David B. Damon, Michael Butters, Robert W. Dugger,
  • Peter Dunn, Sally Gut, Brian P. Jones, Thomas G. LaCour,
  • C. William Murtiashaw, Harry A. Watson Jr., James Weeks,
  • and Timothy D. White
  • 10. A Practical Synthesis of Tetrasubstituted
  • Imidazole p38 MAP Kinase Inhibitors: A New Method
  • for the Synthesis of a-Amidoketones 161
  • Jerry A. Murry, Doug Frantz, Lisa Frey, Arash Soheili,
  • Karen Marcantonio, Richard Tillyer, Edward J.J. Grabowski,
  • and Paul J. Reider
  • 11. Solution Phase Synthesis of the Pulmonary
  • Surfactant KL4: A 21 Amino Acid Synthetic Protein 181
  • Ahmed F. Abdel-Magid, Mary Ellen Bos, Urs Eggmann,
  • Cynthia A. Maryanoff, Lorraine Scott, Adrian Thaler,
  • and Frank J. Villani
  • Indexes
  • Author Index 201
  • Subject Index 203.