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Calibration in analytical science : methods and procedures /

Bibliographic Details
Main Author: Kościelniak, Paweł
Format: eBook
Language:English
Published: Weinheim, Germany : Wiley-VCH, 2023.
Subjects:
Analytical chemistry.
Calibration.
Online Access:Connect to the full text of this electronic book
Table of Contents:
  • Cover
  • Title Page
  • Copyright
  • Contents
  • Preface
  • Chapter 1 Calibration Fundamentals
  • 1.1 Analytical Context
  • 1.2 Principles of Analytical Calibration
  • 1.3 Calibration Standards and Models
  • 1.4 Calibration Procedures and Methods
  • 1.5 Calibration in the Context of Measurement Errors
  • 1.5.1 Uncontrolled Analytical Effects
  • 1.5.2 Elimination and Compensation of Uncontrolled Effects
  • 1.6 Calibration in Qualitative Analysis
  • 1.7 Calibration in Quantitative Analysis
  • 1.8 General Rules for Correct Calibration
  • References
  • Chapter 2 Calibration-Free Analysis
  • 2.1 Novel Approach
  • 2.2 Empirical Calibration
  • 2.3 Theoretical Calibration
  • 2.3.1 Fixed Models
  • 2.3.2 Flexible Models
  • References
  • Chapter 3 Calibration Methods in Qualitative Analysis
  • 3.1 Classification
  • 3.2 External Calibration Methods
  • 3.2.1 External Standard Method
  • 3.2.2 Reference Sample Method
  • 3.3 Internal Calibration Methods
  • 3.3.1 Internal Standard Method
  • 3.3.2 Indirect Method
  • 3.4 Standard Addition Method
  • References
  • Chapter 4 Introduction to Empirical Calibration in Quantitative Analysis
  • 4.1 Classification
  • 4.2 Formulation of Model Functions
  • 4.3 Examination of Interference Effect
  • 4.4 Mathematical Modeling of Real Function
  • References
  • Chapter 5 Comparative Calibration Methods
  • 5.1 External Calibration Methods
  • 5.1.1 External Standard Method
  • 5.1.1.1 Modified Procedures
  • 5.1.2 Dilution Method
  • 5.2 Internal Calibration Methods
  • 5.2.1 Internal Standard Method
  • 5.2.2 Indirect Method
  • References
  • Chapter 6 Additive Calibration Methods
  • 6.1 Basic Aspects
  • 6.2 Standard Addition Method
  • 6.2.1 Extrapolative Variant
  • 6.2.1.1 Modified Procedures
  • 6.2.2 Interpolative Variants
  • 6.2.3 Indicative Variant
  • 6.3 Titration
  • 6.4 Isotope Dilution Method
  • 6.4.1 Radiometric Isotope Dilution
  • 6.4.2 Isotope Dilution Mass Spectrometry
  • 6.4.2.1 Modified Procedures
  • References
  • Chapter 7 Calibration in Nonequilibrium Conditions
  • 7.1 Flow Injection Analysis
  • 7.1.1 Manipulation Techniques
  • 7.1.2 Gradient Technique
  • 7.2 Kinetic Analysis
  • References
  • Chapter 8 Complex Calibration Approaches
  • 8.1 Extrapolative Methods
  • 8.1.1 Extrapolative Indirect Method
  • 8.1.2 Extrapolative Internal Standard Method
  • 8.1.3 Extrapolative Dilution Method
  • 8.2 Mixed Methods
  • 8.3 Combined Methods
  • 8.3.1 Integrated Calibration Methods
  • 8.3.1.1 Simple Integrated Method
  • 8.3.1.2 Complementary Dilution Method
  • 8.3.2 Generalized Calibration Strategy
  • 8.3.2.1 Versatile Flow Injection Calibration Module
  • 8.3.3 Standard Dilution Analysis
  • References
  • Chapter 9 Calibration Approaches for Detection and Examination of Interference Effects
  • 9.1 Introduction
  • 9.2 Simple Procedures for Detection and Examination of Interference Effects
  • 9.3 Detection and Compensation of Additive Interference Effect
  • 9.3.1 Interpolative Procedure
  • 9.3.2 Extrapolative Procedure