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| LEADER |
00000cam a2200000Ii 4500 |
| 001 |
in00000354571 |
| 005 |
20220104090159.0 |
| 008 |
771029s1977 txua bm 000 0 eng d |
| 035 |
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|9 ABN1959AM
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|a (OCoLC)03378192
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|a (OCoLC)3378192
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|a (OCoLC)ocm03378192
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|a TXA
|b eng
|c TXA
|d OCLCQ
|d OCLCF
|d OCLCO
|d OCLCQ
|d TXA
|d UtOrBLW
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| 049 |
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|a TXAM
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| 099 |
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|a 1977
|a Dissertation
|a F585
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| 100 |
1 |
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|a Flannery, John Edward.
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| 245 |
1 |
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|a Diorganylarsinic acids :
|b preparation and use as extractants for gold (III) and uranium (VI) /
|c by John Edward Flannery, Jr.
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| 264 |
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1 |
|a [College Station, Tex.] :
|b Flannery,
|c 1977.
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| 300 |
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|a xv, 122 leaves :
|b illustrations ;
|c 28 cm
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| 336 |
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|a text
|b txt
|2 rdacontent
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| 337 |
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|a unmediated
|b n
|2 rdamedia
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| 338 |
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|a volume
|b nc
|2 rdacarrier
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| 500 |
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|a "Major subject: Chemistry."
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| 500 |
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|a Vita.
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| 502 |
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|c Texas A & M University
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| 504 |
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|a Includes bibliographical references (leaves 117-121).
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| 520 |
3 |
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|a The new compounds dicyclohexylarsinic acid and bis(2-phenyl ethyl)- arsinic acid were prepared in 83% and 50% yields, respectively, as white crystalline materials by reacting diethylaminodichloroarsine with the appropriate Grignard reagents and oxidizing the hydrolyzed reaction mixtures. To prepare ion exchange resins containing RASO₂H- groups, precursor diorganylarsinic compounds with functional groups allowing the formation of polymers are needed. 4-Bromophenyl(methyl)arsinic acid was obtained from diethylamino(methyl)chloroarsine and 4-bromophenylmagnesium bromide. 2-Hydroxyethyl(methyl)arsinic acid has been successfully prepared by the Meyer reaction and purified. 2-Trichlorosiloxyethyl(methyl)iodoarsine was prepared from this arsinic acid as a possible precursor for a polymeric arsinic acid. Attempts to introduce arsinic acid groups into polystyrene by reacting polystyrene-4- diazonium chloride with methyldichioroarsine gave a product with 10% arsenic. This corresponds to the substitution of MeAsO₂H- groups (via arsenic-carbon bonds) in the para position of 1 out of every 5 phenyl rings in the polymer matrix.
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| 650 |
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|a Extraction (Chemistry)
|0 http://id.loc.gov/authorities/subjects/sh85046579
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| 650 |
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|a Organoarsenic compounds.
|0 http://id.loc.gov/authorities/subjects/sh85095535
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| 650 |
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0 |
|a Solvolysis.
|0 http://id.loc.gov/authorities/subjects/sh85124749
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| 650 |
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|a Major chemistry.
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| 650 |
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7 |
|a Extraction (Chemistry)
|2 fast
|0 (OCoLC)fst00919005
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| 650 |
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7 |
|a Organoarsenic compounds.
|2 fast
|0 (OCoLC)fst01047913
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| 650 |
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7 |
|a Solvolysis.
|2 fast
|0 (OCoLC)fst01125697
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| 655 |
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7 |
|a Academic theses.
|2 lcgft
|0 http://id.loc.gov/authorities/genreForms/gf2014026039
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| 700 |
1 |
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|a Irgolic, K. J.,
|e degree supervisor.
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| 700 |
1 |
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|a Zingaro, R.,
|e degree committee member.
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| 710 |
2 |
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|a Texas A & M University,
|e degree granting institution.
|0 http://id.loc.gov/authorities/names/n80125885
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| 856 |
4 |
1 |
|u http://proxy.library.tamu.edu/login?url=http://proquest.umi.com/pqdweb?did=760971471&sid=1&Fmt=2&clientId=2945&RQT=309&VName=PQD
|z Link to ProQuest copy.
|t 0
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| 856 |
4 |
1 |
|u https://hdl.handle.net/1969.1/DISSERTATIONS-362061
|z Link to OAKTrust copy
|t 0
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| 994 |
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|a C0
|b TXA
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| 999 |
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|i 5319aa36-df3b-36aa-9762-051270b5cfa3
|t 0
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| 952 |
f |
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|p noncirc
|a Texas A&M University
|b J.J. Pickle Campus
|c High Density Repository
|s HDR
|d Remote Storage
|t 0
|e 1977 Dissertation F585
|h Other scheme
|i unmediated -- volume
|m A14840984055
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| 952 |
f |
f |
|a Texas A&M University
|b College Station
|c Electronic Resources
|s www_evans
|d Available Online
|t 0
|e 1977 Dissertation F585
|h Other scheme
|
| 998 |
f |
f |
|a 1977 Dissertation F585
|t 0
|l Remote Storage
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| 998 |
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f |
|a 1977 Dissertation F585
|t 0
|l Available Online
|